HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 71252189, compound → HCID 71253194, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 71252189 | HCID 71252189 | — |
| Solvent | Dimethylamine tetrahydrofuran | HCID 22320367 | — |
| Product | HCID 71253194 | HCID 71253194 | 53.9% |
Reaction Steps
Using N,N-di-tert-butyloxycarbonyl-5-(1,1-dioxo-1λ6-isothiazolidin-2-yl)-2-[4-(5-ethyl-3-methylpyridin-2-yl)piperazine-1-carbonyl]benzamide (202 mg) described in Example 785 and 2M dimethylamine tetrahydrofuran solution (180 μL) and by the reaction and treatment in the same manner as in Example 770, the title compound (81 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-49574d12d1bf49fba2a9c7c6f6e477fe |
| Source note | uspto-grants-2014_08 |