HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanesultam → HCID 71252106, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanesultam | HCID 642157 | — |
| Reactant | HCID 71253013 | HCID 71253013 | — |
| Product | HCID 71252106 | HCID 71252106 | 37.2% |
Reaction Steps
Using 1-{5-chloro-2-[4-(3,5-dimethylpyridin-2-yl)piperazine-1-carbonyl]phenyl}-3-methylimidazolidine-2,4-dione (149 mg) described in Preparation Example 256 and isothiazolidine 1,1-dioxide (61 mg) and by the reaction and treatment in the same manner as in Example 666, the title compound (66 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-e1b9981728314ca291ac1cd5b0e879c4 |
| Source note | uspto-grants-2014_08 |