HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 71252306, compound → HCID 71252462, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 71252306 | HCID 71252306 | — |
| Solvent | Dimethylamine tetrahydrofuran | HCID 22320367 | — |
| Product | HCID 71252462 | HCID 71252462 | 45.9% |
Reaction Steps
Using N,N-di-tert-butyloxycarbonyl-2-[4-(3,5-dimethylpyridin-2-yl)piperazine-1-carbonyl]-5-(1,1-dioxo-1λ6-isothiazolidin-2-yl)benzamide (115 mg) described in Example 808 and 2 mol/L dimethylamine tetrahydrofuran solution (105 μL) and by the reaction and treatment in the same manner as in Example 770, the title compound (39 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-2b5a7a527a5c433296b25cce19ce0df4 |
| Source note | uspto-grants-2014_08 |