HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131714074, compound → H-Pro-Trp-Met-NH2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131714074 | HCID 131714074 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | H-Pro-Trp-Met-NH2 | HCID 13306573 | 86.8% |
Reaction Steps
Starting from 3.722 g (7 mmol) of Boc-Pro-Trp-Met-NH2 (VI) and operating as in Step 2 of Example 1, 2.621 g (80% yield) of VII were obtained from absolute ethyl alcohol; [α]D20 =-23.0° (c=1 MeOH); RfC 0.41; E1.2 0.76.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04491541 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-7747a47ad94a47669a06f234635562cd |
| Source note | uspto-grants-1985_01 |