HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 123262017, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Pentane | HCID 8003 | — |
| Reactant | Trichlorosilane | HCID 24811 | — |
| Reactant | Diethoxychlorosilane | HCID 80978 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 123262017 | HCID 123262017 | — |
Reaction Steps
Following the same general procedure described in Example 1, 2 liters of pentane and 404 mls of trichlorosilane were charged in a 5 L flask. During reflux, 464 mls of anhydrous ethanol was added dropwise. After the alcoholysis was completed, 550 mls of dimethylamine was added to the unisolated diethoxychlorosilane. Distillation yielded 290 g of diethoxy(dimethylamino)silane (b.p. 138°-139° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04491669 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-e9cf11db6d9347cf917c42109a56b8eb |
| Source note | uspto-grants-1985_01 |