Benzyl Bromide → HCID 10354744, compound

HRID 2412386Notes

Reaction equation

HRID 2412386 reaction equation
[CH2:1]([O:8][CH2:9][CH:10]([CH2:13][O:14][CH2:15][CH2:16][CH2:17]CCCCCCCCCCCCCC)[CH2:11][OH:12])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH:32](C1OCC(CO)CO1)(C)C.C(Br)C1C=CC=CC=1>>[CH:16]([CH:15]1[O:12][CH2:11][CH:10]([CH2:9][O:8][CH2:1][C:2]2[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=2)[CH2:13][O:14]1)([CH3:17])[CH3:32]

Participants

4

Reactant 3

HCID 7498Benzyl BromideHCID 38684535113-53-2HCID 20432218HCID 20432218, compound

Product 1

HCID 10354744HCID 10354744, compound

Procedure

The 2-benzyloxymethyl-3-heptadecyloxy-1-propanol used as starting material is obtained by reacting 2-isopropyl-5-hydroxymethyl-1,3-dioxan with benzyl bromide to give 2-isopropyl-5-benzyloxymethyl-1,3-dioxan (oil), subsequent splitting with sulfuric acid and reaction with an equimolar amount of heptadecyl bromide.

Workup

  1. customis obtained

Sources & evidence

ORD record
ord-48eb47db5cef441686088b152c9c34ec
Source dataset
uspto-grants-1985_01
Patent number
US04492659

Reaction notes

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