HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propanone, 1-bromo-3-(4-nitrophenyl)- → HCID 13093759, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propanone, 1-bromo-3-(4-nitrophenyl)- | HCID 12232302 | — |
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 13093759 | HCID 13093759 | — |
Reaction Steps
A mixture of 1-bromo-3-(4-nitrophenyl)acetone and potassium phthalimide (7.2 g.) in toluene (100 ml.) was heated under reflux with stirring for 4 hours. The mixture was filtered, the filtrate evaporated. The residue was purified by chromatography on silica gel using CH2Cl2 as eluant to give 1-phthalimido-3-(4-nitrophenyl)acetone, m.p. 184°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04492692 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-c47d263c92f646cfbea3b935dec90581 |
| Source note | uspto-grants-1985_01 |