Methyl Isocyanate → HCID 20432335, compound

Participants

Reaction Steps

4-(2-Aminoethyl)-2-fluoro-1-triphenylmethylimidazole was dissolved in ether, treated with methylisocyanate, and stirred overnight at ambient temperature. Work-up gave 1-[2-(2-fluoro-1-triphenylmethylimidazol-4-yl)ethyl]-3-methylurea, having the following n.m.r. spectrum in CDCl3 : 2.54 (t, 2H); 2.7 (d, 3H); 3.35 (q, 2H); 5.1 (m, 1H); 6.4 (m, 1H); 6.3 (s, 1H); 7.2 (m, 15H).

Provenance & Evidence