HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 4-(3-Ethanesulphonylpropyl)-2-fluoro-1-triphenylmethylimidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 4-(3-Ethanesulphinylpropyl)-2-fluoro-1-triphenylmethylimidazole | HCID 20432420 | — |
| Product | 4-(3-Ethanesulphonylpropyl)-2-fluoro-1-triphenylmethylimidazole | HCID 20432317 | — |
Reaction Steps
Using the same technique as for the starting material of Example 50, but using two equivalents of 3-chloroperbenzoic acid, there was obtained 4-(3-ethanesulphonylpropyl)-2-fluoro-1-triphenylmethylimidazole, having the following n.m.r. in CDCl3 : 1.35 (t, 3H); 2.09 (quintet, 2H); 2.58 (t, 2H); 2.84 (q, 4H); 6.29 (s, 1H); 7.0-7.4 (m, 15H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04492692 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-0de220272dce44cab58481c99229c3d0 |
| Source note | uspto-grants-1985_01 |