HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86651778, compound → HCID 66717306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86651778 | HCID 86651778 | — |
| Reactant | HCID 86651779 | HCID 86651779 | — |
| Product | HCID 66717306 | HCID 66717306 | 53.4% |
Reaction Steps
Reaction and post-treatment were carried out in the same manner as in Example 3-(b) except for using tert-butyl[tert-butoxycarbonyl(6-{(pyridin-2-ylsulfonyl)[4-(thiazol-4-yl)benzyl]aminomethyl}pyridin-2-yl)amino]acetate (230 mg, 0.353 mmol) obtained in Example 16-(a) in place of tert-butyl[tert-butoxycarbonyl(6-{(pyridin-2-ylsulfonyl)[4-(thiazol-2-yl)benzyl]aminomethyl}pyridin-2-yl)amino]acetate to afford the title compound (93.5 mg) as a white solid. (Yield: 53%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08648097B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-3e152130df6b49a4adcc4d63ecc0eaf5 |
| Source note | uspto-grants-2014_02 |