HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 12799928, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 12797226 | HCID 12797226 | — |
| Product | HCID 12799928 | HCID 12799928 | — |
Reaction Steps
A solution of 2-(n-dodecyl)indole-5-carboxylic acid (13.8 g) in ethanol (80 ml) containing a solution of hydrogen chloride gas in ethanol (100 ml of strength 39% w/v) was refluxed for 6 hours. The solid which separated on cooling was collected and was recrystallised from ethanol to give ethyl 2-(n-dodecyl)indole-5-carboxylate (11.2 g), in the form of a buff powder, m.p. 77°-79° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04493843 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-b20333bdff834aa388aeface28176abc |
| Source note | uspto-grants-1985_01 |