HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 23682492, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 12797216 | HCID 12797216 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23682492 | HCID 23682492 | 93.2% |
Reaction Steps
A solution of 2-(n-pentadecyl)indole-6-carboxylic acid (15.0 g) in hot ethanol (100 ml) was treated with a solution of sodium hydroxide (2.0 g) in water (50 ml), and a white precipitate was obtained. The precipitate was recrystallised from aqueous ethanol (1:1) (300 ml) to give sodium 2-(n-pentadecyl)-indole-6-carboxylate (14.8 g), in the form of white crystals, m.p. greater than 340° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04493843 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-4534768c28be4667a5be91c24c743914 |
| Source note | uspto-grants-1985_01 |