HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 70491124, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 70490587 | HCID 70490587 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70491124 | HCID 70491124 | 92.8% |
Reaction Steps
Benzhydryl 7-(2-phenylacetamido)-3-[2-(4-methoxyphenoxy)acetoxymethyl]-3-cephem-4-carboxylate (6.0 g.), phosphorus pentachloride (5.65 g.), pyridine (2.2 g.) and methanol (7.3 ml.) were reacted according to a similar manner to that of Preparation 30 (4) to give benzhydryl 7-amino-3-[2-(4-methoxyphenoxy)acetoxymethyl]-3-cephem-4-carboxylate (4.6 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04493833 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-3d3655707a7743b289134c6ab6c73194 |
| Source note | uspto-grants-1985_01 |