Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Chloropyridine | HCID 7977 | — |
| Reactant | Methyl bromoacetate | HCID 60984 | — |
| Product | HCID 13199808 | HCID 13199808 | 46.4% |
Reaction Steps
A mixture of 2-chloropyridine (16 g) and methyl bromoacetate (72 g) was allowed to stand for one week at room temperature and then heated for 7 hours at 60° C. The resulting precipitates were collected by filtration and washed with diethyl ether to give 1-methoxycarbonylmethyl-2-chloropyridinium bromide (17.43 g), mp. 163° to 165° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04495182 |
|---|
| Source dataset | uspto-grants-1985_01 |
|---|
| ORD ID | ord-8dbb328da2184094a8634363ca05823f |
|---|
| Source note | uspto-grants-1985_01 |
|---|
