HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromobenzylamine hydrochloride → HCID 61401012, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromobenzylamine hydrochloride | HCID 2724096 | — |
| Reactant | Pyridine-3-sulfonyl chloride | HCID 3164136 | — |
| Product | HCID 61401012 | HCID 61401012 | 84% |
Reaction Steps
Reaction and post-treatment were carried out in the same manner as in Reference Example 2-(d) except for using 3-pyridylsulfonyl chloride (300 mg, 1.69 mmol), and using 4-bromobenzylamine hydrochloride (342 mg, 1.54 mmol) in place of (6-phenylpyridazin-3-ylmethyl)amine hydrochloride to afford the title compound (422 mg) as a white solid. (Yield: 84%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08648097B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-24adc40dfafd44d699a5d2f1c4ab01b7 |
| Source note | uspto-grants-2014_02 |