Hydrogen iodide → HCID 135626412, compound

HRID 2413010Notes

Reaction equation

HRID 2413010 reaction equation
[CH3:1][N:2]([CH3:29])[CH2:3][CH2:4][CH2:5][N:6]1[C:12]2[CH:13]=[C:14]([O:17]C)[CH:15]=[CH:16][C:11]=2[C:10]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)=[N:9][C:8]2[CH:25]=[CH:26][CH:27]=[N:28][C:7]1=2.I>C(O)(=O)C>[OH:17][C:14]1[CH:15]=[CH:16][C:11]2[C:10]([C:19]3[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=3)=[N:9][C:8]3[CH:25]=[CH:26][CH:27]=[N:28][C:7]=3[N:6]([CH2:5][CH2:4][CH2:3][N:2]([CH3:1])[CH3:29])[C:12]=2[CH:13]=1

Participants

4

Reactant 2

HCID 24841Hydrogen iodideHCID 20184041HCID 20184041, compound

Product 1

HCID 135626412HCID 135626412, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

The title compound is prepared by reacting 11-[3-(dimethylamino)propyl]-9-methoxy-6-phenyl-11H-pyrido[2,3-b][1,4]benzodiazepine with hydrogen iodide and glacial acetic acid.

Sources & evidence

ORD record
ord-b066016ac676448b83cee4b3cbc4feef
Source dataset
uspto-grants-1985_01
Patent number
US04495183

Reaction notes

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