HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dichloroaniline → 2,3-Dichloroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dichloroaniline | HCID 11844 | — |
| Reactant | 3,4,5-Trichloroaniline | HCID 12469 | — |
| Product | 3-Chloroaniline | HCID 7932 | — |
| Product | 2,3-Dichloroaniline | HCID 11844 | 100% |
Reaction Steps
Example 9 is repeated, the 3,4,5-trichloroaniline being replaced by 2,3-dichloroaniline. After a reaction time of 28 hours under the same conditions, 3-chloroaniline is obtained with a yield of 100% for a degree of conversion of 100% of the 2,3-dichloroaniline. The degree of hydrodechlorination of the solvent is 0.09%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04495368 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-4472cd2055bf496b9feff6592b6049ee |
| Source note | uspto-grants-1985_01 |