HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → Phenol, 4-(3-pyridinyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | 4-(Pyridin-3-yl)aniline | HCID 459522 | — |
| Product | Phenol, 4-(3-pyridinyl)- | HCID 153040 | — |
Reaction Steps
Using the procedure described above, 3-(4'-aminophenyl)pyridine (10.0 g, 0.059 mol) is converted to the phenol. A total of 7.66 g of product is obtained, after chromatography, which is then recrystallized from acetone-hexane to give 6.52 g (65% of theory) of off-white crystals which have as melting point of 202°-203° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04495357 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-b6a38669ca8241aabdfa6fdf801419e6 |
| Source note | uspto-grants-1985_01 |