HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 20430096, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 20430156 | HCID 20430156 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20430096 | HCID 20430096 | — |
Reaction Steps
28.7 g of 4-(2-chloro-2-methyl-propanoyl)-benzophenone and 5.4 g of sodium methoxide are boiled in 120 ml of methanol for 4 hours. After cooling, the mixture is filtered, the filtrate is evaporated and water is added to the residue. The mixture is extracted with ether and, after drying and evaporating the combined extracts, 4-(2methoxy-2-methyl-propanoyl)-benzophenone is obtained as a viscous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04496447 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-85fc8edf76c743e186fe2e7b065ea13a |
| Source note | uspto-grants-1985_01 |