HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 178506339, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Tris(pentafluoroethyl)phosphane | HCID 15809510 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 178506339 | HCID 178506339 | — |
Reaction Steps
A solution of 1.16 g (3.0 mmol) of tris(pentafluoroethyl)phosphine, (C2F5)3PH, in 1,2-dimethoxyethane is treated with an excess (6 mmol) of a 1.5 M solution of NaOH in water. The mixture is stirred at room temperature for 30 min, and the solvent is subsequently removed in vacuo, giving a colourless residue, sodium bis(pentafluoroethyl)phosphinite, (C2F5)2PONa.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08648202B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-58f4381b1b6e4696a438de74806e17dd |
| Source note | uspto-grants-2014_02 |