HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → (3-BROMOBENZYL)DIMETHYLAMINE
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 3-Bromobenzyl bromide | HCID 69979 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | (3-BROMOBENZYL)DIMETHYLAMINE | HCID 4341665 | 80% |
Reaction Steps
Dimethylamine (51.4 g, 1.14 mol) was reacted with 3-bromobenzyl bromide (95 g, 0.38 mol) in benzene at 5° and the mixtue was acidified with hydrochloric acid and the mixture was extracted with aqueous 3N hydrochloric acid. The aqueous extracts were made alkaline with aqueous potassium hydroxide and the oil which separated out was distilled to give 3-bromo-N,N-dimethylbenzylamine (65 g, 80%) b.p. 118°/20 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04496567 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-52b2dd3f106e4e15a3e588899cbbad87 |
| Source note | uspto-grants-1985_01 |