Cysteamine Hydrochloride → HCID 20430490, compound
Reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[CH:6]=[C:7]([CH:10]=[CH:11][CH:12]=1)[CH2:8]O)[CH3:3].[ClH:13].[NH2:14][CH2:15][CH2:16][SH:17]>Cl>[ClH:13].[ClH:13].[CH3:1][N:2]([CH2:4][C:5]1[CH:6]=[C:7]([CH:10]=[CH:11][CH:12]=1)[CH2:8][S:17][CH2:16][CH2:15][NH2:14])[CH3:3]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Equimolar quantities of 3-(dimethylaminomethyl)benzyl alcohol and cysteamine hydrochloride were heated under reflux for 5 hours in 12N aqueous hydrochloric acid and the mixture was evaporated to give 2-[3-(dimethylaminomethyl)benzylthio]ethylamine dihydrochloride.
Workup
- customthe mixture was evaporated
Sources & evidence
- ORD record
- ord-0cf98c4cbfd6488e98c6e498c287a254
- Source dataset
- uspto-grants-1985_01
- Patent number
- US04496567
Reaction notes
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