HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-{6-Oxo-5-[(pyridin-3-yl)methyl]-1,6-dihydropyrimidin-2-yl}nitramide → HCID 20430495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-{6-Oxo-5-[(pyridin-3-yl)methyl]-1,6-dihydropyrimidin-2-yl}nitramide | HCID 12788688 | — |
| Reactant | HCID 12810610 | HCID 12810610 | — |
| Product | HCID 20430495 | HCID 20430495 | — |
Reaction Steps
Reaction of 2-[4-(dimethylaminomethyl)benzylthio]-ethylamine (1.7 g) with 2-nitroamino-5-(3-pyridylmethyl)-4-pyrimidone (1.7 g) in a similar manner to Example 7(iv) gave 2-[2-(4-(dimethylaminomethyl)benzylthio)ethylamino]-5-(3-pyridylmethyl)-4-pyrimidone m.p. 127°-130°. A sample recrystallised a further time from acetonitrile had m.p. 124°-126°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04496567 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-0248233e54ee42969bca799258c75e47 |
| Source note | uspto-grants-1985_01 |