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HRID2413172

反应详情

EQUATION

反应方程式

HRID 2413172 的结构方程式

REACTANTS

反应物

2
结构：COc1cccc(Cc2cnc(SC)[nH]c2=O)c1
HCID12951526

5-[(3-Methoxyphenyl)methyl]-2-(methylthio)-4(3H)-pyrimidinone

C13H14N2O2S

结构：CN(C)Cc1cccc(CSCCN)c1
HCID12952019

未命名化合物

PRODUCTS

生成物

1
结构：COc1cccc(Cc2cnc(NCCSCc3cccc(CN(C)C)c3)[nH]c2=O)c1
HCID20430524

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

Reaction of 2-(3-dimethylaminomethylbenzylthio)ethylamine by heating under reflux for 40 hours in dry pyridine with 5-(3-methoxybenzyl)-2-methylthio-4-pyrimidone gives 2-[2-(3-dimethylaminomethylbenzylthio)ethylamino]-5-(3-methoxybenzyl)-4-pyrimidone.

WORKUP

后处理

  1. temperatureby heating