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HRID2413174

反应详情

EQUATION

反应方程式

HRID 2413174 的结构方程式

REACTANTS

反应物

2
结构：COc1ccnc(Cc2cnc(N[N+](=O)[O-])[nH]c2=O)c1
HCID12783834

未命名化合物

结构：CN(C)Cc1cccc(CSCCN)c1
HCID12952019

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccnc(Cc2cnc(NCCSCc3cccc(CN(C)C)c3)[nH]c2=O)c1
HCID20430542

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Reaction of 2-[3-(dimethylaminomethyl)benzylthio]ethylamine with 2-nitroamino-5-(4-methoxy-2-pyridylmethyl)-4-pyrimidone in refluxing ethanol gives 2-[2-(3-(dimethylaminomethyl)benzylthio)ethylamino]-5-(4-methoxy-2-pyridylmethyl)-4-pyrimidone which when reacted with boron tribromide gives 2-[2-(3-(dimethylaminomethyl)benzylthio)ethylamino]-5(4-hydroxy-2-pyridylmethyl)-4-pyrimidone.