4-Bromobiphenyl → HCID 54452988, compound

HRID 2413299Notes

Reaction equation

Br[C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[CH:4][CH:3]=1.[Cl:14][CH2:15][Si:16](Cl)([Cl:18])[CH3:17].C([Li])CCC>>[C:5]1([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH:6]=[CH:7][C:2]([Si:16]([Cl:18])([CH2:15][Cl:14])[CH3:17])=[CH:3][CH:4]=1

Participants

Reactant 3

HCID 71014-Bromobiphenyl

HCID 73788Dichloro(chloromethyl)methylsilane

HCID 178418339Butyllithium

Product 1

HCID 54452988HCID 54452988, compound

Procedure

The title compound can be prepared by reaction of equimolar quantities of 4-bromobiphenyl, chloromethyldichloro(methyl)silane, and n-butyllithium according to the procedure of Example 3.

Sources & evidence

ORD record: ord-947c4eae2cae4d5c87e4dcdf04f4c606
Source dataset: uspto-grants-1985_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04496551

Reaction notes

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