HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl p-toluenesulfonate → Methyltriphenylphosphonium p-toluenesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl p-toluenesulfonate | HCID 6645 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Product | Methyltriphenylphosphonium p-toluenesulfonate | HCID 18401301 | — |
Reaction Steps
A mixture of 65.57 g (0.25 mol) of triphenylphosphine and 46.56 g (0.25 mol) of methyl p-toluenesulfonate was heated under nitrogen with stirring in a 130°-C. bath for 1 hr. On cooling, a clear, colorless amorphous glass resulted.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04496643 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-852edb4c93d54ba4b46bd6fb35143fe0 |
| Source note | uspto-grants-1985_01 |