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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2413319Generated: November 3, 2026

Methyl p-toluenesulfonate → HCID 20430720, compound

https://huagongshe.com/reaction/2413319

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl p-toluenesulfonateHCID 6645—
ReactantTriphenylstibineHCID 11777—
ProductHCID 20430720HCID 20430720—

Reaction Conditions

Temperature130 °C

Reaction Steps

A mixture of 17.65 g (0.05 mol) of triphenylstibine and 9.31 g (0.05 mol) of methyl p-toluenesulfonate was heated in a 130° C. bath with nitrogen bubbling through the melt for 18 hr. The resulting syrup was cooled to an amorphous glass which was crystallized by treatment with ether. The resultant crystals were collected and dried.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04496643
Source datasetuspto-grants-1985_01
ORD IDord-8320cbeb6e56435d802eb3c8adb0e549
Source noteuspto-grants-1985_01