HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Ethoxycarbonylmethyl)triphenylphosphonium → HCID 53853771, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Ethoxycarbonylmethyl)triphenylphosphonium | HCID 73732 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 13090787 | HCID 13090787 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53853771 | HCID 53853771 | — |
Reaction Steps
36 ml of a 15% strength solution of sodium methylate in methanol were added dropwise, at 20° C., to a suspension of 22.6 g of 3,7-dichloro-8-formylquinoline and 38.4 g of ethoxycarbonylmethyl-triphenyl-phosphonium chloide in 200 ml of ethanol. The mixture was stirred for 3 hours, after which the precipitate was filtered off under suction, washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04717416 |
| Source dataset | uspto-grants-1988_01 |
| ORD ID | ord-0601905ab212409aaa373c77feecf319 |
| Source note | uspto-grants-1988_01 |