Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 13090787 | HCID 13090787 | — |
| Reactant | HCID 86741956 | HCID 86741956 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54127815 | HCID 54127815 | — |
Reaction Steps
36 ml of a 15% strength solution of sodium methylate in methanol were added to 11 g of 3,7-dichloro-8-formylquinoline and 21.6 g of 4-hydroxyacetophenone-triphenylphosphonium chloride in 150 ml of ethanol. The mixture was stirred for 21/2 hours at 20° C., after which 3 ml of glacial acetic acid were added and the precipitate was filtered off under suction, washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04717416 |
|---|
| Source dataset | uspto-grants-1988_01 |
|---|
| ORD ID | ord-e7e2b04f662f42a8a83157e311725dcc |
|---|
| Source note | uspto-grants-1988_01 |
|---|
