Dodecylamine → 1-(Benzothiazol-2-ylthio)-propane-2,3-dicarboxylic acid mono(dodecylamide)
Reaction equation
[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10][CH2:11][CH:12]1[C:17](=[O:18])[O:16][C:14](=[O:15])[CH2:13]1.[CH2:19]([NH2:31])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30]>>[CH2:19]([NH:31][C:17]([CH:12]([CH2:13][C:14]([OH:16])=[O:15])[CH2:11][S:10][C:2]1[S:1][C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=1)=[O:18])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30]Participants
3
Procedure
A mixture of 6.5 parts of 3-(benzothiazol-2-ylthio)-propane-1,2-dicarboxylic anhydride and 4.3 parts of dodecylamine is heated at 55° during 3 hours to give a mixture of the two isomeric mono-dodecylamides as a yellow oil.
Workup
- temperatureis heated at 55° during 3 hours
- customto give
Sources & evidence
- ORD record
- ord-2d92617ec05541d79a693afceb39ad91
- Source dataset
- uspto-grants-1988_01
- Patent number
- US04719036
Reaction notes
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