Dodecylamine → HCID 70410354, compound

HRID 2413530Notes

Reaction equation

HRID 2413530 reaction equation
[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10][CH:11]1[CH2:16][C:15](=[O:17])[O:14][C:12]1=[O:13].[CH2:18]([NH2:30])[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]>C(OCC)C>[CH2:18]([NH:30][C:12](=[O:13])[CH:11]([S:10][C:2]1[S:1][C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=1)[CH2:16][C:15]([OH:14])=[O:17])[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]

Participants

4

Reactant 2

HCID 13583DodecylamineHCID 54519085HCID 54519085, compound

Product 1

HCID 70410354HCID 70410354, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

A mixture of 7 parts of (benzothiazol-2-ylthio)succinic anhydride, 4.8 parts of dodecylamine and 60 parts of diethyl ether is heated at 35° for 3 hours. Filtration of the resulting mixture gives a mixture of the two isomeric mono(dodecylamides), melting at 117°-121°.

Workup

  1. temperatureis heated at 35° for 3 hours
  2. filtrationFiltration of the resulting mixture
  3. customgives

Sources & evidence

ORD record
ord-db98db27c0d74fea8c83e1454d372b83
Source dataset
uspto-grants-1988_01
Patent number
US04719036

Reaction notes

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