Cyclohexylamine → HCID 70410985, compound

Participants

Reaction Steps

18.5 parts of diethyl 3-(benzothiazol-2-ylthio)-propane- 1,2-dicarboxylate are stirred with 31.1 parts cyclohexylamine for 12 hours at 95° C. The mixture is cooled and toluene added with stirring. The resulting solid is filtered off, washed with toluene and dried to give N,N'-dicyclohexyl 3-(benzothiazol-2-ylthio)-1,2-propane dicarboxylic acid diamide, melting at 147°-49° C.

Provenance & Evidence