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HRID2413678

反应详情

EQUATION

反应方程式

HRID 2413678 的结构方程式

REACTANTS

反应物

2
结构：S=C=Nc1ccccc1
HCID7673

Isothiocyanic acid, phenyl ester

C7H5NS

结构：COc1ccc(C2=NN(c3ccccc3)C(c3ccc(N)cc3)C2)cc1
HCID20155091

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(C2=NN(c3ccccc3)C(c3ccc(NC(=S)Nc4ccccc4)cc3)C2)cc1
HCID20155092

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

3.4 g of 5-(4-aminophenyl)-3-(4-methoxyphenyl)-1-phenyl-2-pyrazoline and 1.5 g of phenyl isothiocyanate were reacted with each other in acetonitrile, and the product was reprecipitated from dimethylformamidemethanol to obtain 2.7 g of the desired end compound.

WORKUP

后处理

  1. customthe product was reprecipitated from dimethylformamidemethanol
  2. customto obtain 2.7 g of the desired end compound