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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2413702Generated: October 31, 2026

HCID 54487808, compound → HCID 54390892, compound

https://huagongshe.com/reaction/2413702

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 54487808HCID 54487808—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 54390892HCID 5439089297.4%

Reaction Steps

In 10 ml of methanol was dissolved 450 mg of compound (11) and 45 mg of 10% Pd-C was added to the solution followed by catalytic hydrogenation at ambient temperature under an atmospheric pressure of hydrogen. The catalyst was filtered off and the solvent was removed by distillation under reduced pressure to obtain 258 mg of (S)-1-methyl-4-oxo-2-azetidinecarboxylic acid (12).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04719207
Source datasetuspto-grants-1988_01
ORD IDord-d486b7cdbee54fd58211f266dc427ea4
Source noteuspto-grants-1988_01