HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54487808, compound → HCID 54390892, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54487808 | HCID 54487808 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54390892 | HCID 54390892 | 97.4% |
Reaction Steps
In 10 ml of methanol was dissolved 450 mg of compound (11) and 45 mg of 10% Pd-C was added to the solution followed by catalytic hydrogenation at ambient temperature under an atmospheric pressure of hydrogen. The catalyst was filtered off and the solvent was removed by distillation under reduced pressure to obtain 258 mg of (S)-1-methyl-4-oxo-2-azetidinecarboxylic acid (12).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04719207 |
| Source dataset | uspto-grants-1988_01 |
| ORD ID | ord-d486b7cdbee54fd58211f266dc427ea4 |
| Source note | uspto-grants-1988_01 |