HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54137886, compound → HCID 53923542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54137886 | HCID 54137886 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53923542 | HCID 53923542 | 94.1% |
Reaction Steps
In 20 ml of methanol was dissolved 1.05 g of compound (16) and 100 mg of 10% Pd-C was added to the solution followed by catalytic hydrogenation at ambient temperature under atmospheric pressure of hydrogen. The catalyst was filtered off and the solvent was removed by distillation under reduced pressure to obtain 650 mg of (S)-1-formyloxymethyl-4-oxo-2-azetidinecarboxylic acid (17).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04719207 |
| Source dataset | uspto-grants-1988_01 |
| ORD ID | ord-79ece012461e41c0967a66b9042578aa |
| Source note | uspto-grants-1988_01 |