HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentanal → 1-[2-Fluoro-4-(trifluoromethyl)phenyl]pentan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentanal | HCID 8063 | — |
| Reactant | 4-Bromo-3-fluorobenzotrifluoride | HCID 142414 | — |
| Product | 1-[2-Fluoro-4-(trifluoromethyl)phenyl]pentan-1-one | HCID 66883012 | — |
Reaction Steps
The titled compound was prepared from 1-bromo-2-fluoro-4-(trifluoromethyl)benzene (200 mg, 0.823 mmol) and valeraldehyde (0.05 mL, 0.8 mmol) in a procedure similar to that of Example 9 (1) as a pale yellow oil (114 mg, yield 97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08648208B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-60915907a5d54c8e94139f16747a5d93 |
| Source note | uspto-grants-2014_02 |