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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2413833Generated: November 1, 2026

HCID 54540367, compound → HCID 20155611, compound

https://huagongshe.com/reaction/2413833

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 54540367HCID 54540367—
SolventHydrochloric AcidHCID 313—
ProductHCID 20155611HCID 2015561141.1%

Reaction Conditions

Temperature90 °C

Reaction Steps

A mixture of 0.935 g (2.17 mmol) of the compound of Example 2 and 20 ml of 6N HCl is stirred at 90° C. for 4 hours. After cooling, the mixture is concentrated under reduced pressure. The residue is triturated with cold ethanol to furnish 0.334 g (41.1%) of title compound as a tan solid:

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04719302
Source datasetuspto-grants-1988_01
ORD IDord-b1821cff399744dc9fa82ed48273a12b
Source noteuspto-grants-1988_01