HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → Ethyl 4-acetoxyacetoacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl 4-chloroacetoacetate | HCID 69484 | — |
| Solvent | (+-)-2-Butanol | HCID 6568 | — |
| Product | Ethyl 4-acetoxyacetoacetate | HCID 11480907 | — |
Reaction Steps
71 ml of ethyl 4-chloro-3-oxobutyrate are reacted with 57 ml of acetic acid and 132 ml of triethylamine in 1 l of 2-butanol by the procedure described in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04720572 |
| Source dataset | uspto-grants-1988_01 |
| ORD ID | ord-f6b421cc26244dbd8e6ba71f1e066481 |
| Source note | uspto-grants-1988_01 |