HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic Acid → Ethyl 4-(benzyloxy)-3-oxobutanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic Acid | HCID 243 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl 4-chloroacetoacetate | HCID 69484 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Ethyl 4-(benzyloxy)-3-oxobutanoate | HCID 9813448 | — |
Reaction Steps
71 ml of ethyl 4-chloro-3-oxobutyrate are reacted with 121.4 g of benzoic acid and 132 ml of triethylamine in 1 l of toluene by the procedure described in Example 4. After removal of the solvent by distillation, the residue is a virtually pure product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04720572 |
| Source dataset | uspto-grants-1988_01 |
| ORD ID | ord-24ad28a59a1a41bfb405481bb6a228b3 |
| Source note | uspto-grants-1988_01 |