HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 54376602, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methoxyacetic Acid | HCID 12251 | — |
| Reactant | Ethyl 4-chloroacetoacetate | HCID 69484 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54376602 | HCID 54376602 | — |
Reaction Steps
71 ml of ethyl 4-chloro-3-oxo-butyrate are reacted with 89.5 g of methoxyacetic acid and 132 ml of triethylamine in 1 l of toluene by the procedure described in Example 4. The product is purified by bulb tube distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04720572 |
| Source dataset | uspto-grants-1988_01 |
| ORD ID | ord-87a2a1276b0340ebabdffbeb7fd8fee5 |
| Source note | uspto-grants-1988_01 |