Triethylamine → HCID 54376602, compound

HRID 2413991Notes

Reaction equation

HRID 2413991 reaction equation
Cl[CH2:2][C:3](=[O:10])[CH2:4][C:5]([O:7][CH2:8][CH3:9])=[O:6].[CH3:11][O:12][CH2:13][C:14]([OH:16])=[O:15].C(N(CC)CC)C>C1(C)C=CC=CC=1>[CH3:11][O:12][CH2:13][C:14]([O:16][CH2:2][C:3](=[O:10])[CH2:4][C:5]([O:7][CH2:8][CH3:9])=[O:6])=[O:15]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 12251Methoxyacetic AcidHCID 69484Ethyl 4-chloroacetoacetate

Product 1

HCID 54376602HCID 54376602, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

71 ml of ethyl 4-chloro-3-oxo-butyrate are reacted with 89.5 g of methoxyacetic acid and 132 ml of triethylamine in 1 l of toluene by the procedure described in Example 4. The product is purified by bulb tube distillation.

Workup

  1. customThe product is purified by bulb tube
  2. distillationdistillation

Sources & evidence

ORD record
ord-87a2a1276b0340ebabdffbeb7fd8fee5
Source dataset
uspto-grants-1988_01
Patent number
US04720572

Reaction notes

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