HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-2-methyl-1,3-propanediol → 1,3-Propanediol, 2-((8-fluoranthenylmethyl)amino)-2-methyl-, hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-2-methyl-1,3-propanediol | HCID 1531 | — |
| Reactant | 773U82 Hydrochloride | HCID 3024572 | — |
| Reactant | 8-Fluoranthenecarboxaldehyde | HCID 11436155 | — |
| Product | 1,3-Propanediol, 2-((8-fluoranthenylmethyl)amino)-2-methyl-, hydrochloride | HCID 150409 | — |
Reaction Steps
Using the reductive amination procedure outlined in 1D, 8-fluoranthenecarbaldehyde (1C) and 2-methyl-2-amino-1,3-propanediol (Aldrich) gave 2-((8-fluoranthenylmethyl)amino)-2-methyl-1,3-propanediol hydrochloride mp 233°-234.5° (dec), (CH3OH/Et2O), (C, H, Cl, N).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04720587 |
| Source dataset | uspto-grants-1988_01 |
| ORD ID | ord-285d186b51e84451b4c554fc48568c72 |
| Source note | uspto-grants-1988_01 |