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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2414074Generated: November 1, 2026

4-Bromobutyronitrile → HCID 20153795, compound

https://huagongshe.com/reaction/2414074

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-BromobutyronitrileHCID 21412—
ReactantHCID 11770746HCID 11770746—
SolventDimethylformamideHCID 6228—
ProductHCID 20153795HCID 20153795—

Reaction Conditions

Temperature60 °C

Reaction Steps

2.47 g of 3-amino-4,6-diphenylpyridazine are dissolved in 5 ml of dimethylformamide, and 1.63 g of 4-bromobutyronitrile are added. The mixture is heated at 60° C. for 2 hours and left to cool. The crystals formed are filtered off and recrystallised from isopropanol. Melting point=202°-204° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04721711
Source datasetuspto-grants-1988_01
ORD IDord-db14b143d50a4b56b89754337be87ff3
Source noteuspto-grants-1988_01