HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formamide, N-[2-[3-(methylthio)phenyl]ethyl]- → 3,4-Dihydro-6-(methylthio)isoquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formamide, N-[2-[3-(methylthio)phenyl]ethyl]- | HCID 10976389 | — |
| Reactant | N-[2-(3-Methoxyphenyl)ethyl]formamide | HCID 13562936 | — |
| Product | 3,4-Dihydro-6-(methylthio)isoquinoline | HCID 11019405 | 13.3% |
Reaction Steps
A procedure identical to that described for the preparation of N-[2-(3-methoxy-phenyl)-ethyl]-formamide in Example 1 was followed using N-[2-(3-methylsulfanyl-phenyl)-ethyl]-formamide (6.7 g, 34 mmol) to give the desired product (0.8 g, 13%). MS: 178.1 (M+1+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06812228B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-a0d458abc5884a77a9867c0b8aad4925 |
| Source note | uspto-grants-2004_11 |