HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → 2-Chlorobenzoyl isocyanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 2-Chlorobenzamide | HCID 69111 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Chlorobenzoyl isocyanate | HCID 9942311 | — |
Reaction Steps
2-Chlorobenzamide was dissolved in dichloromethane, mixed with 1.5 eq. of oxalyl chloride and heated to reflux for 16 hours. The reaction mixture was concentrated under high vacuum and reacted in stage b without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06812250B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-60e4d6686d774ac7a0ecdf1fe5091626 |
| Source note | uspto-grants-2004_11 |