化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Hydrochloric Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | 3-(Boc-aminoethyloxy)benzonitrile | HCID 10989079 | — |
| 溶媒 | 1,4-Dioxane | HCID 31275 | — |
| 生成物 | Hydrochloric Acid | HCID 313 | — |
| 生成物 | 210963-99-8 | HCID 22645198 | — |
反応手順
1.41 g of 3-[2-(t-butoxycarbonylamino)ethoxy]benzonitrile was dissolved in 20 ml of 4 N solution of hydrogen chloride in dioxane, and the obtained solution was stirred at room temperature for 2 hours. The solvent was evaporated, and the residue was suspended in dichloromethane. The obtained suspension was filtered to obtain hydrochloride of the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06812231B2 |
| 出典データセット | uspto-grants-2004_11 |
| ORD ID | ord-8a60ea40610349a38ebc7396ee787deb |
| 出典メモ | uspto-grants-2004_11 |