Hydrochloric Acid → Hydrochloric Acid

HRID 2414436노트

반응식

HRID 2414436 반응식
C(OC([NH:8][CH2:9][CH2:10][O:11][C:12]1[CH:13]=[C:14]([CH:17]=[CH:18][CH:19]=1)[C:15]#[N:16])=O)(C)(C)C.[ClH:20]>O1CCOCC1>[ClH:20].[ClH:20].[NH2:8][CH2:9][CH2:10][O:11][C:12]1[CH:13]=[C:14]([CH:17]=[CH:18][CH:19]=1)[C:15]#[N:16]

참가 물질

5

반응물 2

HCID 313Hydrochloric AcidHCID 109890793-(Boc-aminoethyloxy)benzonitrile

생성물 2

HCID 313Hydrochloric AcidHCID 22645198210963-99-8

시약·촉매·용매 1

HCID 312751,4-Dioxane용매

실험 절차

1.41 g of 3-[2-(t-butoxycarbonylamino)ethoxy]benzonitrile was dissolved in 20 ml of 4 N solution of hydrogen chloride in dioxane, and the obtained solution was stirred at room temperature for 2 hours. The solvent was evaporated, and the residue was suspended in dichloromethane. The obtained suspension was filtered to obtain hydrochloride of the title compound.

후처리

  1. customThe solvent was evaporated
  2. filtrationThe obtained suspension was filtered

출처 및 근거

ORD 기록
ord-8a60ea40610349a38ebc7396ee787deb
출처 데이터셋
uspto-grants-2004_11
특허 번호
US06812231B2

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