Dichloromethane → HCID 69802348, compound

Participants

Reaction Steps

To a solution of methyl[(tert-butoxycarbonyl)amino]{4-[2-(1-pyrrolidinyl)-ethoxy]phenyl}acetate was dissolved in dichloromethane, hydrogen chloride gas was bubbled in for 5 minutes. The reaction was then stirred at room temperature for 0.5 h. The solvent was removed to provide 1.80 g of methyl amino{4-[2-(1-pyrrolidinyl)ethoxy]phenyl}acetate dihydrochloride as a light pink solid Yield ˜100%. mp 80° C. (d). Electrospray Mass Spec 279.2 (M+H)+.

Provenance & Evidence