HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-5-ethoxypyridine → 3-(5-Ethoxy-3-pyridyl)-3,7-diazabicyclo[3.3.0]octane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-5-ethoxypyridine | HCID 11521128 | — |
| Reactant | Octahydropyrrolo(3,4-c)pyrrole | HCID 21867666 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | 3-(5-Ethoxy-3-pyridyl)-3,7-diazabicyclo[3.3.0]octane | HCID 9878002 | — |
Reaction Steps
Obtainable by stirring a mixture of 3-chloro-5-ethoxypyridine (1 eq.), 3.7-Diazabicyclo[3.3.0]octane (1 eq.), potassium-tert-butoxide (2 eq.) and 1.2-dimethoxyethane as solvent. Workup-procedure A/B.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06815438B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-2dda6bea92294f008dfb36b26676ca27 |
| Source note | uspto-grants-2004_11 |